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Upload photos to your account or other selected accounts.Sensitive determination of strychnine in serum and urine with a split-flow system-based microchip based on Fe3O4@SiO2 magnetic nanoparticles.
A novel preconcentration strategy for the determination of strychnine based on a split-flow system-based microchip with Fe3O4@SiO2 magnetic nanoparticles (MNPs) as an adsorbent was developed. Under optimum conditions, the amounts of strychnine adsorbed from the sample solution onto the MNPs can be calculated as 2.63±0.03 and 3.36±0.03ng per μL, respectively. The detection limit of strychnine was 0.1ngmL-1. Several experimental parameters were systematically investigated and optimized. Compared to the other methods for the determination of strychnine in biological samples, the proposed method exhibited a wide linear range of 0.5-60ngmL-1, low detection limit (0.1ngmL-1), high enrichment factor (110), and acceptable recoveries (81.4-91.4%). Compared with the traditional single-channel analysis, split-flow based microchip offers a further enhanced mass transfer and enrichment of analytes and also more possibility of analysis. The split-flow based microchip method was successfully applied to the determination of strychnine in serum and urine samples. The results provided reliable evidence of the reliability and efficiency of the proposed method in determining strychnine in biological samples.Q:
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… very much interested in exploring opportunities to work together, on projects or as friends.. I am fortunate to be able to afford a house with a small garden and am friendly with.. I have had one friend from the UK who was an I-. I met this girl through football practice in Glasgow and we began to see each other everyday after school.. I would love to return home in a few months. . 1.3.2.2.1.20.2.1.14.4.1.15.12.1.16.2.1.27.2.1.2.2.3.1.3.1.2.1.6.4.2.1.14.16.1.26.2.1.19.4.1.18.6.1.18.3.1.7.4.2.1.19.3.2.3.4.4.2.1.5.3.0.4.2.1.2.2.6.1.1.1.1.1.16.1.1.5.2.3.5.2.1.0.8.1.1.2.1.1.1.1.2.4.0.4.0.9.1.0.2.5.1.0.4.0.1.0.2.0.8.1.1.1.1.1.4.0.3.0.3.0.9.0.2.1.4.0.4.0.6.0.8.0.3.1.0.1.0.4.0.6.0.1.0.7.0.7.1.1.4.0.3.0.0.9.0.2.1.0.2.1.0.8.0.3.1.1.4.1.1.15.10.0.0.0.0.0.1.0.0.0.1.0.0.1.0.1.0.0.0.0.0.
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